Infrared spectra of phthalic acid, the hydrogen phthalate ion, and the phthalate ion in aqueous solution

Loring, JS; Karlsson, M; Fawcett, WR; Casey, WH

HERO ID

1596875

Reference Type

Journal Article

Year

2001

Language

English

PMID

11471716

HERO ID 1596875
In Press No
Year 2001
Title Infrared spectra of phthalic acid, the hydrogen phthalate ion, and the phthalate ion in aqueous solution
Authors Loring, JS; Karlsson, M; Fawcett, WR; Casey, WH
Journal Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy
Volume 57
Issue 8
Page Numbers 1635-1642
Abstract The infrared spectra of a series of aqueous solutions containing phthalic acid (1,2-benzenedicarboxylic acid) and varying pH were examined using attenuated total reflection Fourier transform infrared spectroscopy and potentiometry. The basis spectra of phthalic acid, the hydrogen phthalate ion, and the phthalate ion were isolated using a factor analysis in which the absorbance of these species varies with pH and total phthalate concentration according to equilibrium and mass balance relations. Assignments of these basis spectra were made by comparison with spectra calculated ab initio. The conditional formation constants of phthalic acid and the hydrogen phthalate ion were determined at 25.0 +/- 0.1 degreesC in 0.6 M NaCl ionic media using infrared spectroscopy and in 1.5 M NaCl ionic media using both infrared spectroscopy and potentiometry. (C) 2001 Elsevier Science B.V. All rights reserved.
Doi 10.1016/S1386-1425(01)00391-2
Pmid 11471716
Wosid WOS:000169725600011
Url https://linkinghub.elsevier.com/retrieve/pii/S1386142501003912
Is Certified Translation No
Dupe Override No
Comments Source: Web of Science WOS:000169725600011
Is Public Yes
Language Text English
Keyword phthalate; hydrogen phthalate; phthalic acid; infrared spectroscopy; factor analysis