Coprecipitation of gold(III), palladium(II) and lead(II) for their flame atomic absorption spectrometriceterminations

Soylak, M; Tuzen, M

HERO ID

165816

Reference Type

Journal Article

Year

2008

Language

English

PMID

17703875

HERO ID 165816
In Press No
Year 2008
Title Coprecipitation of gold(III), palladium(II) and lead(II) for their flame atomic absorption spectrometriceterminations
Authors Soylak, M; Tuzen, M
Journal Journal of Hazardous Materials
Volume 152
Issue 2
Page Numbers 656-661
Abstract An enrichment-separation procedure basedn the coprecipitationf gold(III), palladium(II) and lead(II)ons with nickel(II)-5-methyl-4-(2-thiazolylazo) resorcinol complex has beeneveloped. The analytical parametersncluding pH, amountsf 5-methyl-4-(2-thiazolylazo) resorcinol, sample volume, etc. wasnvestigated for quantitative recoveriesf Au(III), Pd(II) and Pb(II). Interferenceue to various cations and anions has also beennvestigated. Theetection limits for analyteons by 3sigma were 2.6 microg L(-1) for lead, 1.5 microg L(-1) for gold, 2.1 microg L(-1) for palladium. The accuracyf the method was evaluated by the analysisf certified reference materials (NIST SRM 2711 Montana soil, GBW 07309 Stream sediment). The proposed procedure was successfully applied to environmental samples for theeterminationsf analytes.
Doi 10.1016/j.jhazmat.2007.07.027
Pmid 17703875
Wosid WOS:000254765100024
Is Certified Translation No
Dupe Override No
Is Public Yes
Language Text English
Keyword Gold/solation & purification; Lead/solation & purification; Nickel; Palladium/solation & purification; Precipitation; Soil Pollutants/solation & purification; Spectrophotometry, Atomic; Water Pollutants, Chemical/solation & purification
Is Qa No
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