Rate of solvent extraction of chromium(III) in aqueous solutions with 2-thenoyltrifluoroacetone into chloroform

Yamada, M; Honda, N; Takasugi, R; Sekine, T

HERO ID

1972033

Reference Type

Journal Article

Year

1999

HERO ID 1972033
In Press No
Year 1999
Title Rate of solvent extraction of chromium(III) in aqueous solutions with 2-thenoyltrifluoroacetone into chloroform
Authors Yamada, M; Honda, N; Takasugi, R; Sekine, T
Volume 6
Page Numbers 41-50
Abstract The rate of solvent extraction of chromium(III) in aqueous nitrate solutions which contained 2-thenoyltrifluoroacetone(Htta), acetate buffer and ascorbic acid has been studied. The aqueous solution prepared was left standing for varying time intervals before agitation with chloroform. The chromium(III) complex extracted was then measured. The amount of chromium(III) extracted was larger when hydrated Cr3+ was initially present in the aqueous solution than when chromium(III) was produced by reduction of chromium(VI) in the aqueous solution. The extracted complex was assumed to be tris(thenoyltrifluoroacetonato)chromium(III) by spectrophotometry. This was quite different from extraction with acetylacetone which formed the extractable complex more rapidly when the chromium(III) was produced by reduction of chromium(VI) than when it was initially added in the form of hydrated Cr3+. The extraction with Htta proceeded more quickly when complex formation with this extractant took place in the aqueous phase followed by chloroform extraction than when the extractant is initially present in the chloroform and the aqueous solution containing chromium(III) was immediately agitated with the solvent.
Wosid WOS:000085274900005
Is Certified Translation No
Dupe Override No
Comments Journal:SOLVENT EXTRACTION RESEARCH AND DEVELOPMENT-JAPAN 1341-7215
Is Public Yes