Effects of alcohols and diols on the phase behaviour of quaternary systems

Alany, RG; Rades, T; Agatonovic-Kustrin, S; Davies, NM; Tucker, IG

HERO ID

3037506

Reference Type

Journal Article

Year

2000

Language

English

PMID

10699705

HERO ID 3037506
In Press No
Year 2000
Title Effects of alcohols and diols on the phase behaviour of quaternary systems
Authors Alany, RG; Rades, T; Agatonovic-Kustrin, S; Davies, NM; Tucker, IG
Journal International Journal of Pharmaceutics
Volume 196
Issue 2
Page Numbers 141-145
Abstract The aim of the current study was to investigate the effect of different co-surfactants on the phase behaviour of the pseudoternary system water:ethyl oleate:nonionic surfactant blend (sorbitan monolaurate/polyoxyethylene 20 sorbitan mono-oleate). Four aliphatic alcohols (1-propanol, 1-butanol, 1-hexanol and 1-octanol) and four 1,2-alkanediols (1,2-propanediol. 1,2-pentanediol, 1,2-hexanediol and 1,2-octanediol) were used. The co-surfactant-free system forms two different colloidal structures, a water-in-oil microemulsion (w/o ME) and lamellar liquid crystals (LC) and two coarse dispersions, water-in-oil (w/o EM) and oil-in-water (o/w EM) emulsions. Microemulsion region area (%ME), liquid crystalline region area (%LC), amount of amphiphile blend required to produce a balanced microemulsion (%AMPH) and amount of water solubilised (%W)were used as assessment criteria to evaluate the co-surfactants. Seven calculated physico-chemical descriptors were used to represent the different co-surfactants. 1-butanol, 1,2-hexanediol and 1,2-octanediol produced balanced MEs capable of solubilising a high percentage of both oil and water. A similarity was observed between the descriptors attributed to I-butanol and 1,2-hexanediol. The requirements of a co-surfactant molecule to produce a balanced microemulsion were: HLB Value 7.0-8.0, a carbon backbone of 4-6 atoms, percentage carbon of 60-65%, percentage oxygen of 20-30%, log P value 0.2-0.9 and log 1/S (S: aqueous solubility) close to zero. (C) 2000 Elsevier Science B.V. All rights reserved.
Doi 10.1016/S0378-5173(99)00408-1
Pmid 10699705
Wosid WOS:000085847200004
Is Certified Translation No
Dupe Override No
Is Public Yes
Language Text English
Keyword microemulsions; cosurfactants; alcohols; diols; phase diagrams