HOMOGENEOUS-CATALYTIC ACETOXYLATION OF 1-HEXENE AND CYCLOHEXENE

Trushova, NV; Devekki, AV

HERO ID

4684045

Reference Type

Journal Article

Year

1992

HERO ID 4684045
In Press No
Year 1992
Title HOMOGENEOUS-CATALYTIC ACETOXYLATION OF 1-HEXENE AND CYCLOHEXENE
Authors Trushova, NV; Devekki, AV
Journal Petroleum Chemistry
Volume 32
Issue 4
Page Numbers 313-319
Abstract A study has been made of the acetoxylation of 1-hexene and cyclohexene in the presence of PdCl42- and a nitrate-iodate reoxidative system ensuring high yields of the corresponding acetoxyalkanes. It has been established that a binuclear pi-olefinic bridge-type palladium complex is a catalytically active particle. It is assumed that the mechanisms of formation of 1,2-hexanediol monoacetate and diacetoxycyclohexane differ at the final stage of transformation of the acetoxonium ion. Acetoxylation is retarded by the reaction products, which screen the coordination sphere of palladium.
Wosid WOS:A1992KE92200011
Is Certified Translation No
Dupe Override No
Is Public Yes