Reverisble thermal gelation of soft semi-crystalline polyethylene microparticles with surface interactions in squalane

Ling, GH; Shaw, MT

HERO ID

4972305

Reference Type

Journal Article

Year

2008

HERO ID 4972305
In Press No
Year 2008
Title Reverisble thermal gelation of soft semi-crystalline polyethylene microparticles with surface interactions in squalane
Authors Ling, GH; Shaw, MT
Journal Polymer Engineering and Science
Volume 48
Issue 2
Page Numbers 329-335
Abstract The effect of temperature on the steady-shear viscosity of a soft semi-crystalline crosslinked-polyethylene microparticle suspension in squalane was studied using rotational rheometry. The results show a sharp increase in the viscosity of the system occurring at about 86 degrees C. The magnitude of this spike is dependent on the concentration of the suspension and is reproducible over multiple heating and cooling cycles. This phenomenon has been attributed to the melting of the crystalline regions within the particles, causing them to swell by soaking up squalane. The Mooney equation was used to model the viscosity data based on swelling data obtained from separate experiments. The results showed that the model is inadequate for describing the observed phenomenon, suggesting the possibility of additional interactions existing among the particles. POLYM. ENG. SCI., 48:329-335, 2008. (c) 2007 Society of Plastics Engineers.
Doi 10.1002/pen.20933
Wosid WOS:000252792500015
Is Certified Translation No
Dupe Override No
Is Public Yes