Xanthine oxidase catalyzed oxidation of aldehydes Oxidation of aliphatic aldehydes and 2- and 4-pyridinecarboxaldehyde

Gregory, D; Goodman, PA; Meany, JE

HERO ID

7132

Reference Type

Journal Article

Year

1972

Language

English

PMID

4347179

HERO ID 7132
In Press No
Year 1972
Title Xanthine oxidase catalyzed oxidation of aldehydes Oxidation of aliphatic aldehydes and 2- and 4-pyridinecarboxaldehyde
Authors Gregory, D; Goodman, PA; Meany, JE
Journal Biochemistry
Volume 11
Issue 24
Page Numbers 4472-4477
Abstract The xanthine oxidase catalyzed oxidations of a series of aliphatic aldehydes and 2- and 4-pyridinecarboxaldehydes were studied in phosphate buffers by monitoring the reduction of ferricytochrome c at 25.0° In aqueous solutions, these aldehydes exist in equilibrium with their hydrated forms. In order to clearly establish the relationship between the acid-base-catalyzed hydration of the aldehydes and the enzymatically catalyzed oxidation of the aldehyde-hydrate system, detailed kinetic analyses of both processes were carried out separately. Enzymatic catalysis was studied as a function of pH and of acetaldehyde concentration, and the catalytic components associated with the acid-base-catalyzed hydration of acetaldehyde in phosphate buffers were evaluated. These data, taken together, show not only that the unhydrated aldehyde is the substrate for xanthine oxidase action but also suggest that substantial enzymatic inhibition arises from the formation of the hydrate. The involvement of the unhydrated aldehyde as the preferential substrate is commnn for the aldehydes studied and in the evaluation of their respective Michaelis constants, Km: acetaldehyde, 0.0058 m; propionaldehyde, 0.014 μ; n-butyraldehyde, 0.048 m; 2-pyridinecarboxaldehyde, 0.0061 m; and 4-pyridinecarboxaldehyde, 0.002 m; correction was made to compensate for respective fractions of hydration. © 1972, American Chemical Society. All rights reserved.
Doi 10.1021/bi00774a008
Pmid 4347179
Wosid WOS:A1972O008500008
Url https://www.scopus.com/inward/record.uri?eid=2-s2.0-0015519047&doi=10.1021%2fbi00774a008&partnerID=40&md5=dec4046e67da5228752bdab916a1d4b9
Is Certified Translation No
Dupe Override No
Comments Biochemistry 11: 4472-4477.
Is Public Yes
Language Text English
Is Qa No